The formation of hitherto disputed monophasic vanadium antimonate is reported and its thermally induced decomposition into β-Sb2 O4 containing ca. 5% vanadium is associated with a new low-temperature stabilisation of this phase; on further heating the hexagonal ‘β-Sb2O4’ plate-type crystals develop crystalline outgrowths of vanadium antimonate.
F. J. Berry, M. E. Brett and W. R. Patterson, J. Chem. Soc., Chem. Commun., 1982, 695 DOI: 10.1039/C39820000695
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