The (–)-(R)-dienone (13) was prepared in 10 steps from the known 8-hydroxy-5-methoxy-2, 3-dihydronaphthalen-1(4H)-one (2), and the chirality at C(7) in (13) corresponds to that found at C(9) in the naturally occurring anthracyclines related to daunomycin.
R. N. Warrener, P. S. Gee and R. A. Russell, J. Chem. Soc., Chem. Commun., 1981, 1100 DOI: 10.1039/C39810001100
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