Nickel-catalysed addition of deuterium cyanide to (E)-1-deuterio-3,3-dimethylbut-1-ene (1) and subsequent analysis of the dideuteriated nitrile (2) by 1H n.m.r. spectroscopy shows that the addition of deuterium and cyanide occurs in a cis-fashion.
Jan-E. Bäckvall and O. S. Andell, J. Chem. Soc., Chem. Commun., 1981, 1098 DOI: 10.1039/C39810001098
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