SCHEDULED MAINTENANCE
In dimethyl sulphoxide–NaHCO3, 16α-aminomethyl- and 16α-benzylaminomethyl-3-methoxy-17β-tosyloxyestra-1,3,5(10)-triene undergo cyclisation into the corresponding tetrahydro-oxazin-2-ones instead of oxidation.
G. Schneider, L. Hackler and G. Dombi, J. Chem. Soc., Chem. Commun., 1980, 891 DOI: 10.1039/C39800000891
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