13 C N. m. r. has been shown to be a further valuable tool for investigating the position of silylation in trimethylsilylated secondary amides. Whereas most lactams are N-silylated and 2-hydroxypyridines O-silylated, acetanilides exist as a mixture of isomers.
S. A. Matlin, P. G. Sammes and R. M. Upton, J. Chem. Soc., Perkin Trans. 1, 1979, 2478 DOI: 10.1039/P19790002478
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