cis- and trans-1-Trimethylsilyl-pent-3-en-1-yne, -hex-3-en-1-yne, and -hept-3-en-1-yne have been prepared by fractional distillation of their cis–trans-mixtures and shown to provide a convenient route for the synthesis of the corresponding stereoisomeric terminal acetylenes.
I. W. Farrell, M. T. W. Hearn and V. Thaller, J. Chem. Soc., Perkin Trans. 1, 1978, 1485 DOI: 10.1039/P19780001485
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