Functionalisation of the angular methyl group of the tetrahydrosantonin (1) was achieved by a method involving, as the key step, the photochemical oxidation of the bromohydrin (7) derived thereform, subsequently leading to compound (3) and (10).
M. Watanabe and A. Yoshikoshi, J. Chem. Soc., Chem. Commun., 1978, 748 DOI: 10.1039/C39780000748
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