A new synthetic method for the preparation of high molecular weight fluorocarbon ethers has been developed; polyethylene oxide was caused to react with elemental fluorine under conditions carefully regulated to fragment and perfluorinate the polyether system and yield a number of new fluorocarbon ethers.
G. E. Gerhardt and R. J. Lagow, J. Chem. Soc., Chem. Commun., 1977, 259 DOI: 10.1039/C39770000259
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