The formation of trithiametacyclophanes from the trisodium salt of a tris(mercaptoalkyl)benzene and a trisbromoalkylmethane is described. 1H N.m.r. spectra were used to determine the structures of the products, with the aid of shift reagents.
A. Ricci, R. Danieli and S. Rossini, J. Chem. Soc., Perkin Trans. 1, 1976, 1691 DOI: 10.1039/P19760001691
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