Acid-catalysed monobutylidenation of 1-deoxy-D-galactitol (l-fucitol) yields the diastereoisomeric 2,3-acetals under kinetic control. The main product under thermodynamic control is the 4,6-acetal; the 4,5-acetal (4% yield) was also isolated.
T. G. Bonner, E. J. Bourne, D. Lewis and L. Yüceer, J. Chem. Soc., Perkin Trans. 1, 1975, 1323 DOI: 10.1039/P19750001323
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