The formation, 220 MHz 1H n.m.r. spectrum, and the X-ray crystal structure of the first bicyclic phosphazene are described; the P–N bond lengths are typically those of a phosphazene except at the bridgehead where they are significantly longer.
T. S. Cameron, Kh. Mannan, S. S. Krishnamurthy, A. C. Sau, A. R. V. Murthy, R. A. Shaw and M. Woods, J. Chem. Soc., Chem. Commun., 1975, 975 DOI: 10.1039/C39750000975
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