Issue 3, 1975
From the journal:

Journal of the Chemical Society, Chemical Communications

The cyclotetramerisation of dimethyl acetylenedicarboxylate and the x-ray structure of [pd{h(c8(co2me)8)}cl(pyridine)2], an unusual five-co-ordinate palladium(ii) complex

Alfred Konietzny,   Pamela M. Bailey  and  Peter M. Maitlis  

Abstract

Reaction of dimethyl acetylenedicarboxylate with PdCl2 in methanol yields [Pd{HC8(CO2Me)8}Cl]2, which gives monomeric and non-conducting adducts [Pd{HC8(CO2Me)8}ClL2]; an X-ray structure determination of the adduct (L = pyridine) shows it to contain five-co-ordinate PdII.

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Article information

DOI
https://doi.org/10.1039/C39750000078
Article type
Paper

J. Chem. Soc., Chem. Commun., 1975, 78-79

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The cyclotetramerisation of dimethyl acetylenedicarboxylate and the x-ray structure of [pd{h(c8(co2me)8)}cl(pyridine)2], an unusual five-co-ordinate palladium(ii) complex

A. Konietzny, P. M. Bailey and P. M. Maitlis, J. Chem. Soc., Chem. Commun., 1975, 78 DOI: 10.1039/C39750000078

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