The absorption spectrum of single crystals of Rh(CO)2(acac) in polarised i.r. tight has enabled direct and unambiguous differentiation of in-plane from out-of-plane modes.
D. M. Adams and W. R. Trumble, J. Chem. Soc., Dalton Trans., 1974, 690 DOI: 10.1039/DT9740000690
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