Homoallylic alcohols can be dehydrated under exceptionally mild conditions by conversion into their thiobenzoate O-esters and irradiation between –70° and room temperature. A variety of substrates have been dehydrated by this method.
D. H. R. Barton, M. Bolton, P. D. Magnus, K. G. Marathe, G. A. Poulton and P. J. West, J. Chem. Soc., Perkin Trans. 1, 1973, 1574 DOI: 10.1039/P19730001574
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