The preparation of some new dissymmetric alkyl compounds of tin(IV) is described, in particular those containing t-butyl and t-pentyl groups. The 1H n.m.r. spectra of these compounds at 100 and 220 MHz has been investigated, and the appearance of magnetic non-equivalence is discussed. A temperature-dependence study of the 1H n.m.r. spectra confirms that the tetra-alkyltin(IV) compounds are stereochemically stable.
K. S. A. Kandil and C. E. Holloway, J. Chem. Soc., Dalton Trans., 1973, 1421 DOI: 10.1039/DT9730001421
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