The reaction systems RCl + R′PCl2+ MClx(R = t-butyl, R′= chloride or methyl) have been investigated with the metal halides NbCl5, TaCl5, and WCl6. In each case, complexes of the type (RR′PCl2)(MVCl6) have been characterised by vibrational spectroscopy. Magnetic susceptibility measurements are reported for the tungsten complexes.
J. I. Bullock, F. W. Parrett and N. J. Taylor, J. Chem. Soc., Dalton Trans., 1973, 522 DOI: 10.1039/DT9730000522
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