The use of heteronuclear noise decoupling combined with the observation of the 13C and 13C-satellite spectra enable the chemical shifts and coupling constants of all the magnetic nuclei in 1,1,1,4,4-hexafluorobutane to be obtained; these show that the compound exists entirely as the trans-rotamer in solution.
R. J. Abraham and P. Loftus, J. Chem. Soc., Chem. Commun., 1973, 454 DOI: 10.1039/C39730000454
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