Solvation numbers have been determined for a number of lanthanide shift reagents with three substances, using low-temperature 1H n.m.r. spectroscopy under conditions where chemical exchange is slow.
D. F. Evans and M. Wyatt, J. Chem. Soc., Chem. Commun., 1973, 339 DOI: 10.1039/C39730000339
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