Issue 0, 1972

Total syntheses of (–)-O-methylandrocymbine, (–)-kreysigine, and alkaloid CC-10 methyl ether

Abstract

(–)-O-Methylandrocymbine (1) was obtained from (–)-1-(2-bromo-3,4,5-trimethoxyphenethyl)-1,2,3,4-tetrahydro-7-hydroxy-6-methoxy-2-methylisoquinoline (13a) by irradiation. The corresponding (+)-phenolic bromoisoquinoline (13b) gave alkaloid CC-10 methyl ether [(+)-O-methylandrocymbine](3) and (–)-kreysigine (6).

Article information

Article type
Paper

J. Chem. Soc., Perkin Trans. 1, 1972, 2160-2162

Total syntheses of (–)-O-methylandrocymbine, (–)-kreysigine, and alkaloid CC-10 methyl ether

T. Kametani, Y. Satoh and K. Fukumoto, J. Chem. Soc., Perkin Trans. 1, 1972, 2160 DOI: 10.1039/P19720002160

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