Decoupling of phosphorus–hydrogen spin–spin interactions upon addition of paramagnetic complexing reagents of the first transition series to phosphorus-containing esters has been investigated by 31P n.m.r. spectroscopy. Attempts at complete phosphorus–hydrogen decoupling by use of non-co-ordinating paramagnetic reagents were unsuccessful.
R. Engel and L. Gelbaum, J. Chem. Soc., Perkin Trans. 1, 1972, 1233 DOI: 10.1039/P19720001233
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