Copper vapour has been shown to react with boron trichloride on condensation at low temperatures to give good yields of diboron tetrachloride. The method has been developed into a laboratory preparation of diboron tetrachloride on a 10 g scale.
P. L. Timms, J. Chem. Soc., Dalton Trans., 1972, 830 DOI: 10.1039/DT9720000830
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