The Raman spectra (2000–2200 cm–1) of aqueous solutions of [M(CN)5]3–(M = Ni or Co) together with complementary i.r. data suggest that both anions have a square-based pyramidal arrangement of cyanide ligands.
W. P. Griffith and J. R. Lane, J. Chem. Soc., Dalton Trans., 1972, 158 DOI: 10.1039/DT9720000158
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