N-Trimethylsilylamides are oxidized by diperoxo-oxohexamethylphosphoramidomolybdenum(VI) to give the corresponding hydroxamic acids, which are initially isolated as their MoVI complexes, but which can be liberated by treatment with ethylenediaminetetra-acetic acid (EDTA).
S. A. Matlin and P. G. Sammes, J. Chem. Soc., Chem. Commun., 1972, 1222 DOI: 10.1039/C39720001222
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