Contrary to predictions based on spectroscopic evidence, the crystal structure of the [VO(C2O4)2H2O]2– anion has a distorted octahedral arrangement of oxygen atoms about vanadium with a cis-arrangement of oxalate groups and a co-ordinated water molecule.
G. E. Form, E. S. Raper, R. E. Oughtred and H. M. M. Shearer, J. Chem. Soc., Chem. Commun., 1972, 945 DOI: 10.1039/C39720000945
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