The structure (IV) of the C16H16·Fe3(CO)9 complex derived from iron tricarbonyl complexes of dimers of cyclo-octatetraene has been shown to contain a vinyl radical to which one of the iron atoms in an Fe2(CO)6 group forms a π-bond while the other is σ-bonded; this result corrects an earlier structural assignment.
A. H.-J. Wang, I. C. Paul and G. N. Schrauzer, J. Chem. Soc., Chem. Commun., 1972, 736 DOI: 10.1039/C39720000736
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