When silica bearing creatain chemisorbed silanes is heated to a high temperatrure in vacuo, the chemisorbed layer is disrupted and the surface of the silica is modified; surface =SiH2 groups are formed and the silica surface becomes unusually reactive.
M. J. D. Low, M. Shimizu and J. C. McManus, J. Chem. Soc. D, 1971, 579b DOI: 10.1039/C2971000579B
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