Formation of similar amounts of cis- and trans-σ-but-2-enyl pentacyanocobaltate(III) and of syn-π-(1-methylallyl)tetracyanocobaltate(III) in the hydrogenation of butadiene by pentacyanocobaltate(II) is demonstrated from the i.r. spectrum and the n.m.r. spectra at 60, 100, and 220 MHz.
T. Funabiki and K. Tarama, J. Chem. Soc. D, 1971, 1177 DOI: 10.1039/C29710001177
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