A new phosphate synthesis (suitable for highly hindered phosphates) is described, based on the reaction of an alkoxy-radical (generated by nitrite photolysis) with a trialkyl, or other appropriate, phosphite.
D. H. R. Barton, T. J. Bentley, R. H. Hesse, F. Mutterer and M. M. Pechet, J. Chem. Soc. D, 1971, 912 DOI: 10.1039/C29710000912
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