1 H N.m.r. studies at 100 MHz show that for 4-methoxycyclohexanone in benzene solution at 31°, the axial : equatorial population ratio is 3:1; the chair conformation in which the methoxy-group is axial predominates contrary to the conclusion previously deduced from dipole moment studies.
R. D. Stolow and T. W. Giants, J. Chem. Soc. D, 1971, 528 DOI: 10.1039/C29710000528
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