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Mass spectral and 1H n.m.r. evidence, coupled with degradation of bufotalin to 3β-acetoxybufotalien (II), in turn prepared by total synthesis, provide unequivocal support for the assignment of structure (I) to bufotalin.
G. R. Pettit, P. Brown, F. Bruschweiler and L. E. Houghton, J. Chem. Soc. D, 1970, 1566 DOI: 10.1039/C29700001566
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