The X-ray crystal structure of CsB9H14 shows the presence of three BH2 groups and two B–H–B groups in the open face of the B9 cluster: in solution, the 11B(28·87 MHz) and 1H(220 MHz) n.m.r. spectra indicate pseudo-threefold symmetry with nine terminal B–H bonds and five more labile hydrogen atoms.
N. N. Greenwood, H. J. Gysling, J. A. McGinnety and J. D. Owen, J. Chem. Soc. D, 1970, 505 DOI: 10.1039/C29700000505
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