Homo- and hetero-nuclear double resonance experiments are used to facilitate the complete analysis of the n.m.r. spectra of C6F5Z (Z = CHO, CH3, and CF3). An accurate relation is presented between the 19F and 1H resonant frequencies in C6F6 and tetramethylsilane respectively. A novel decoupling method is described for the measurement of very small coupling constants, and is applied to C6F5·CH3.
R. R. Dean and W. McFarlane, J. Chem. Soc. B, 1969, 509 DOI: 10.1039/J29690000509
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