Hexuloses and heptuloses are identified on g.l.c. or t.l.c. by the products of two-step trimethylsilylation whose initial product is, or contains, the trimethylsilyl ether in which the hemiacetal hydroxy-group is free.
T. Okuda and K. Konishi, J. Chem. Soc. D, 1969, 796 DOI: 10.1039/C29690000796
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