Aluminium chloride-catalysed acetylation of aluminium(III) trisacetylacetonate leads to the exclusive formation of a diacylated product. The same ketone can similarly be obtained directly from acetylacetone. Ferric chloride-catalysed acetylation of iron(III) trisacetylacetonate or acetylacetone gives low yields of 2,6-dimethyl-4-pyrone.
P. C. Doolan and P. H. Gore, J. Chem. Soc. C, 1967, 211 DOI: 10.1039/J39670000211
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