Far-infrared spectra and two-dimensional X-ray single crystal data show that tungsten pentachloride has a bridged dimeric octahedral structure like Mo2Cl10, and does not contain trimeric clusters [W3Cl12]3+[Cl–]3 as previously suggested.
P. M. Boorman, N. N. Greenwood, M. A. Hildon and H. J. Whitfield, J. Chem. Soc. A, 1967, 2017 DOI: 10.1039/J19670002017
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