The proton magnetic resonance spectra of the group 5 trisilyls are reported, including the satellite spectra due to 29Si at natural abundance. A double resonance experiment shows that the two 29SiH coupling constants in P(SiH3)3 have the same sign. The phosphorus spectrum of the latter is described, and J(29SiP) tentatively assigned.
E. A. V. Ebsworth and G. M. Sheldrick, Trans. Faraday Soc., 1966, 62, 3282 DOI: 10.1039/TF9666203282
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