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An automated repeating batch with catalyst recycle approach to nitro group hydrogenolysis

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Abstract

An automated repeating batch approach has been developed for the rapid screening and scale up of a nitroaromatic to aniline catalytic hydrogenolysis. Advantages of this approach include the ability to scale up in small equipment using readily available powdered catalysts, rapid reaction kinetics due to high catalyst to substrate ratio, lower overall catalyst use, high throughput from a small reactor, and the ability to refresh the catalyst without manual intervention.

Graphical abstract: An automated repeating batch with catalyst recycle approach to nitro group hydrogenolysis

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Publication details

The article was received on 04 Jan 2017, accepted on 13 Feb 2017, published on 13 Feb 2017 and first published online on 13 Feb 2017


Article type: Communication
DOI: 10.1039/C7RE00002B
Citation: React. Chem. Eng., 2017, Advance Article
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    An automated repeating batch with catalyst recycle approach to nitro group hydrogenolysis

    K. P. Cole, M. D. Johnson, M. E. Laurila and J. R. Stout, React. Chem. Eng., 2017, Advance Article , DOI: 10.1039/C7RE00002B

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