Issue 35, 2017
From the journal:

Organic & Biomolecular Chemistry

Total syntheses and configuration assignments of JBIR-04 and unantimycin A†

Yoshinosuke Usuki, ORCID logo *a   Chie Hamadaa  and  Tetsuya Satoh ORCID logo a  

* Corresponding authors

a Department of Chemistry, Graduate School of Science, Osaka City University, 3-3-138 Sugimoto, Sumiyoshi-ku, Osaka 558-8585, Japan
E-mail: usuki@sci.osaka-cu.ac.jp

Abstract

First total syntheses of JBIR-04 and unantimycin A have been achieved. Comparison of our spectroscopic data with those reported for natural samples verified the structure of the natural products; (2S,4S,6S,7R,9S,28S) configuration was thus assigned via total synthesis.

Graphical abstract: Total syntheses and configuration assignments of JBIR-04 and unantimycin A

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Article information

DOI
https://doi.org/10.1039/C7OB01732D
Article type
Paper
Submitted
14 Jul 2017
Accepted
12 Aug 2017
First published
14 Aug 2017

Org. Biomol. Chem., 2017,15, 7346-7351

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Total syntheses and configuration assignments of JBIR-04 and unantimycin A

Y. Usuki, C. Hamada and T. Satoh, Org. Biomol. Chem., 2017, 15, 7346 DOI: 10.1039/C7OB01732D

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