Issue 100, 2013
From the journal:

Chemical Communications

Enhanced shape stability of Pd–Rh core–frame nanocubes at elevated temperature: in situ heating transmission electron microscopy†

Ning Lu,a   Jinguo Wang,a   Shuifen Xie,b   Younan Xiabc  and  Moon J. Kim*ad  

* Corresponding authors

a Department of Materials Science and Engineering, The University of Texas at Dallas, Richardson, TX 75080, USA
E-mail: moonkim@utdallas.edu
Fax: +1-972-883-5725
Tel: +1-972-883-6635

b The Wallace H. Coulter Department of Biomedical Engineering, Georgia Institute of Technology and Emory University, Atlanta, GA 30332, USA

c School of Chemistry and Biochemistry and School of Chemical and Biomolecular Engineering, Georgia Institute of Technology, Atlanta, GA 30332, USA

d Department of Nanobio Materials and Electronics, World Class University, Gwangju Institute of Science and Technology, Gwangju 500-712, Korea

Abstract

Shape stability of Pd–Rh core–frame nanocubes was studied by in situ heating transmission electron microscopy. Pd–Rh nanocubes could maintain cubic shape at elevated temperature compared with pure Pd. The surface diffusion process of Rh onto {100} side surfaces is believed to postpone the degradation to higher temperature.

Graphical abstract: Enhanced shape stability of Pd–Rh core–frame nanocubes at elevated temperature: in situ heating transmission electron microscopy

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Article information

DOI
https://doi.org/10.1039/C3CC46465B
Article type
Communication
Submitted
23 Aga 2013
Accepted
15 Okt 2013
First published
17 Okt 2013

Chem. Commun., 2013,49, 11806-11808

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Enhanced shape stability of Pd–Rh core–frame nanocubes at elevated temperature: in situ heating transmission electron microscopy

N. Lu, J. Wang, S. Xie, Y. Xia and M. J. Kim, Chem. Commun., 2013, 49, 11806 DOI: 10.1039/C3CC46465B

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