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Abstract | Cited by

C–H arylation with heterogeneous palladium was investigated. The surface oxidation of Pd nanoparticles with a hypervalent iodine reagent, [Ph2I]BF4, resulted in the generation of Pd(II)–aryl–oxo clusters, which were characterized as the crucial intermediate.

Graphical abstract: Characterization of heterogeneous aryl–Pd(ii)–oxo clusters as active species for C–H arylation

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