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Abstract | Cited by

Reaction of the first homoleptic U(III) guanidinate complex with diphenyldiazomethane results in two-electron oxidation of U(III) to U(V) and isolation of a U(V) hydrazido complex. Corresponding U(V) imido, U(V) oxo, and U(IV) azido complexes were also synthesized for structural comparison.

Graphical abstract: Two-electron oxidation of a homoleptic U(iii) guanidinate complex by diphenyldiazomethane

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