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Abstract | Cited by

Upon heating, lithium L-malate undergoes topotactic dehydration to form a phase containing the unsaturated fumarate ligand, in which the original 3-D framework remains intact. Insight into this unusual transformation has been obtained by single crystal X-ray diffraction, MAS-NMR, in situ powder X-ray diffraction and DFT calculations.

Graphical abstract: Topotactic elimination of water across a C–C ligand bond in a dense 3-D metal–organic framework

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