Issue 22, 2016

Facile synthesis of an organically-derivatized hexavanadate containing the remote amino group, TBA2[V6O13{(OCH2)3CNH2}2]

Abstract

An effective synthetic strategy for the amino-containing organic derivative of hexavanadate, TBA2[V6O13{(OCH2)3CNH2}2], is presented. By using this method, the yield is increased extremely and crystals of the intermediate and cation-exchanged products are both obtained and structurally characterized via single-crystal X-ray diffraction, IR and 1H-NMR.

Graphical abstract: Facile synthesis of an organically-derivatized hexavanadate containing the remote amino group, TBA2[V6O13{(OCH2)3CNH2}2]

Supplementary files

Article information

Article type
Communication
Submitted
23 dec 2015
Accepted
05 feb 2016
First published
05 feb 2016

CrystEngComm, 2016,18, 4042-4045

Facile synthesis of an organically-derivatized hexavanadate containing the remote amino group, TBA2[V6O13{(OCH2)3CNH2}2]

A. Bayaguud, K. Chen and Y. Wei, CrystEngComm, 2016, 18, 4042 DOI: 10.1039/C5CE02534F

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