Direct observations of the MOF (UiO-66) structure by transmission electron microscopy

Liangkui Zhu; Daliang Zhang; Ming Xue; Huan Li; Shilun Qiu

doi:10.1039/C3CE41122B

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Direct observations of the MOF (UiO-66) structure by transmission electron microscopy†

Liangkui Zhu,^a Daliang Zhang,*^a Ming Xue,^a Huan Li^a and Shilun Qiu*^a

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* Corresponding authors

^a State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, Jilin University, Changchun, Jilin 130012, P.R. China
E-mail: zhangdaliang@jlu.edu.cn, sqiu@jlu.edu.cn
Fax: +86 431 5168589
Tel: +86 431 5168589

Abstract

As a demonstration of ab initio structure characterizations of nano metal organic framework (MOF) crystals by high resolution transmission electron microscopy (HRTEM) and electron diffraction tomography methods, a Zr-MOF (UiO-66) structure was determined and further confirmed by Rietveld refinements of powder X-ray diffraction. HRTEM gave direct imaging of the channels.

This article is part of the themed collection: Structural Design of Coordination Polymers

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Article information

DOI: https://doi.org/10.1039/C3CE41122B
Article type: Communication
Submitted: 12 jun 2013
Accepted: 19 avg 2013
First published: 19 avg 2013

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CrystEngComm, 2013,15, 9356-9359

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Direct observations of the MOF (UiO-66) structure by transmission electron microscopy

L. Zhu, D. Zhang, M. Xue, H. Li and S. Qiu, CrystEngComm, 2013, 15, 9356 DOI: 10.1039/C3CE41122B

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CrystEngComm

Direct observations of the MOF (UiO-66) structure by transmission electron microscopy†

Abstract

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Direct observations of the MOF (UiO-66) structure by transmission electron microscopy

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