Online GPC monitoring for batch and flow polymerisation reactions

William Pointer, Rowan Radmall, Owen Tooley, James Town, Dennis C. J. Haggart, Zhichun Zhai, Xiaofan Yang, Daniel W. Lester, Paul Wilson and David M. Haddleton

Polym. Chem., 2025, 16, 3329
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Broadband ultrafast 2D NMR spectroscopy for online monitoring in continuous flow

Célia Lhoste, Margherita Bazzoni, Justine Bonnet, Aurélie Bernard, François-Xavier Felpin, Patrick Giraudeau and Jean-Nicolas Dumez

Analyst, 2023, 148, 5255
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Fast and accurate diffusion NMR acquisition in continuous flow

Isabel A. Thomlinson, Matthew G. Davidson, Catherine L. Lyall, John P. Lowe and Ulrich Hintermair

Chem. Commun., 2022, 58, 8242
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From at-line to online NMR: coupling probe-based autosampler with benchtop NMR

Yining Ji, Zhihao Lin, Latevi Lawson, François Lévesque, David A. Foley, Robert Espina and Hector Robert

React. Chem. Eng., 2023, 8, 2270
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Catalyst speciation and deactivation in the ruthenium-mediated transformation of ethynyl-β-ionol to α,β-unsaturated esters for vitamin A synthesis

Asad Saib, Roman Goy, Jonathan Medlock, Bettina Wüstenberg, Gabriele Kociok-Köhn, Catherine L. Lyall, John P. Lowe and Ulrich Hintermair

Catal. Sci. Technol., 2025, 15, 355
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Mapping catalyst activation, turnover speciation and deactivation in Rh/PPh3-catalysed olefin hydroformylation

Alejandro Bara-Estaún, Catherine L. Lyall, John P. Lowe, Paul G. Pringle, Paul C. J. Kamer, Robert Franke and Ulrich Hintermair

Catal. Sci. Technol., 2022, 12, 5501
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Automated approaches, reaction parameterisation, and data science in organometallic chemistry and catalysis: towards improving synthetic chemistry and accelerating mechanistic understanding

Stuart C. Smith, Christopher S. Horbaczewskyj, Theo F. N. Tanner, Jacob J. Walder and Ian J. S. Fairlamb

Digital Discovery, 2024, 3, 1467
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Autonomous reaction self-optimization using in-line high-field NMR spectroscopy

Nour El Sabbagh, Margherita Bazzoni, Yuliia Horbenko, Aurélie Bernard, Daniel Cortés-Borda, Patrick Giraudeau, François-Xavier Felpin and Jean-Nicolas Dumez

React. Chem. Eng., 2024, 9, 2599
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Convenient and accurate insight into solution-phase equilibria from FlowNMR titrations

Daniel B. G. Berry, Ian Clegg, Anna Codina, Catherine L. Lyall, John P. Lowe and Ulrich Hintermair

React. Chem. Eng., 2022, 7, 2009
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Theoretical analysis of flow effects in spatially encoded diffusion NMR

Rituraj Mishra and Jean-Nicolas Dumez

The Journal of Chemical Physics, 2023, 158
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In‐line Multidimensional NMR Monitoring of Photochemical Flow Reactions

Margherita Bazzoni, Célia Lhoste, Justine Bonnet, Kouakou Eric Konan, Aurélie Bernard, Patrick Giraudeau, François‐Xavier Felpin and Jean‐Nicolas Dumez

Chemistry A European J, 2023, 29
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Flow‐Chemistry‐Enabled Synthesis of 5‐Diethylboryl‐2,3′‐bipyridine and Its Self‐Assembly Dynamics

Shigeharu Wakabayashi, Masahiro Takumi, Shintaro Kamio, Masayuki Wakioka, Yasuhiro Ohki and Aiichiro Nagaki

Chemistry A European J, 2023, 29
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Fast Multidimensional Flow Nuclear Magnetic Resonance at High Field for Real‐Time Reaction Monitoring and Flow Synthesis

Margherita Bazzoni, Yuliia Horbenko, Nour El Sabbagh, Achille Marchand, Magdalena Grochowska‐Tatarczak, Aurélie Bernard, Patrick Giraudeau, François‐Xavier Felpin and Jean‐Nicolas Dumez

Chemistry Methods, 2025, 5
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Online Reaction Monitoring with Fast and Flow‐Compatible Diffusion NMR Spectroscopy

Achille Marchand, Rituraj Mishra, Aurélie Bernard and Jean‐Nicolas Dumez

Chemistry A European J, 2022, 28
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Preparation of Sulfonyl Chlorides by Oxidative Chlorination of Thiols and Disulfides using HNO3/HCl/O2 in a Flow Reactor

Niklas Sulzer, Dominik Polterauer, Christopher A. Hone and C. Oliver Kappe

ChemSusChem, 2024, 17
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In‐Situ Investigations of Polyoxometalate‐Catalysed Biomass Oxidation to Formic Acid by Using Multinuclear High Resolution Flow NMR Spectroscopy

Jan‐Dominik H. Krueger, Maximilian J. Poller, Catherine Lyall, John Lowe, Ulrich Hintermair and Jakob Albert

ChemCatChem, 2024, 16
DOI: 10.1002/cctc.202400402

MaDDFLOSY(Mass Determination via Diffusion in FLow Ordered SpectroscopY) for the Determination of Diffusion-Averaged Molecular Weight of Polymers in Continuous Motion Using Benchtop NMR

William Pointer, Owen Tooley, Asad Saib, Rowan Radmall, Paul Wilson, Daniel Lester, James Town, Robin J. Blagg and David Haddleton

Macromolecules, 2025, 58, 5201
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A Simple Device for Automated Mixing of Heterogeneous Solid‐Liquid Reactions During In‐Situ Monitoring by NMR Spectroscopy

Yuan Gao, Andrew M. R. Hall, Nicole A. Fohn, Edward J. King, Lloyd A. L. Mitchell, George A. Steedman and Guy C. Lloyd‐Jones

Eur J Org Chem, 2024, 27
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Low-Field Flow 31P NMR Spectroscopy for Organometallic Chemistry: On-Line Analysis of Highly Air-Sensitive Rhodium Diphosphine Complexes

Laura Tadiello, Hans-Joachim Drexler and Torsten Beweries

Organometallics, 2022, 41, 2833
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Flow-NMR as a Process-Monitoring Tool for mRNA IVT Reaction

Aritra Sarkar, Guogang Dong, Jennifer Quaglia-Motta and Kelly Sackett

Journal of Pharmaceutical Sciences, 2024, 113, 900
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Clean 1H NMR Spectra of Products Directly from Batch and Flow Reaction Mixtures

Yuliia Horbenko, Martin Jaudronnet, Nour El Sabbagh, Margherita Bazzoni, Aurélie Bernard, Mathias Nilsson, Patrick Giraudeau, François‐Xavier Felpin and Jean‐Nicolas Dumez

ChemistryEurope, 2025, 3
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A Tale of Two Designs: Comparing Design of Experiment Strategies for Reaction Optimization

Linda Romano, Veronica Ceccucci, Leonardo Tensi, Claudio Santi and Luca Sancineto

Chemistry Methods, 2025
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Reaction monitoring via benchtop nuclear magnetic resonance spectroscopy: A practical comparison of on‐line stopped‐flow and continuous‐flow sampling methods

Tristan Maschmeyer, David J. Russell, José G. Napolitano and Jason E. Hein

Magnetic Reson in Chemistry, 2024, 62, 310
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Understanding Rh‐catalysed Hydroformylation with Phosphite Ligands through Catalyst Speciation Analysis by Operando FlowNMR Spectroscopy

Alejandro Bara‐Estaún, Catherine L. Lyall, John P. Lowe, Paul G. Pringle, Paul C. J. Kamer, Robert Franke and Ulrich Hintermair

ChemCatChem, 2023, 15
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Paramagnetic Relaxation Agents for Enhancing Temporal Resolution and Sensitivity in Multinuclear FlowNMR Spectroscopy

Alejandro Bara‐Estaún, Marie C. Harder, Catherine L. Lyall, John P. Lowe, Elizaveta Suturina and Ulrich Hintermair

Chemistry A European J, 2023, 29
DOI: 10.1002/chem.202300215