Issue 10, 2021

The extraction of phenolic acids and polysaccharides from Lilium lancifolium Thunb. using a deep eutectic solvent

Abstract

Establishing a fast and effective extraction method for herbs is beneficial for the determination of their main compounds and estimating their quality. In this study, deep eutectic solvents (DESs) were optimized to simultaneously extract three main types of phenolic acids, i.e., regaloside B, regaloside C, and regaloside E, and polysaccharides from the bulbs of Lilium lancifolium Thunb. Based on the optimized extraction conditions, i.e., an extraction temperature of 50 °C, an extraction time of 40 min, a solid–liquid ratio of 1 : 25, and a ratio of water in the DES of 20%, the extracted amounts of regaloside B, regaloside C, and regaloside E reached 0.31 ± 0.06 mg g−1, 0.29 ± 0.03 mg g−1, and 3.04 ± 0.38 mg g−1, respectively. The extraction efficiencies were higher than those obtained using conventional organic solvents. Next, the polysaccharide levels were measured and compared with those obtained using a conventional hot water extraction method, and equivalent extraction efficiencies were obtained with the conventional hot water extraction method. This study provides a new application of deep eutectic solvents (DESs) for simultaneously extracting phenolic acids and polysaccharides from the bulbs of L. lancifolium Thunb. Considering the biodegradability and pharmaceutical acceptability, DESs as a class of green solvents could have wide applications in the extraction of natural products.

Graphical abstract: The extraction of phenolic acids and polysaccharides from Lilium lancifolium Thunb. using a deep eutectic solvent

Article information

Article type
Paper
Submitted
29 des 2020
Accepted
04 feb 2021
First published
09 feb 2021

Anal. Methods, 2021,13, 1226-1231

The extraction of phenolic acids and polysaccharides from Lilium lancifolium Thunb. using a deep eutectic solvent

L. Chen, Y. Yang, R. Zhou, L. Fang, D. Zhao, P. Cai, R. Yu, S. Zhang and J. Huang, Anal. Methods, 2021, 13, 1226 DOI: 10.1039/D0AY02352C

To request permission to reproduce material from this article, please go to the Copyright Clearance Center request page.

If you are an author contributing to an RSC publication, you do not need to request permission provided correct acknowledgement is given.

If you are the author of this article, you do not need to request permission to reproduce figures and diagrams provided correct acknowledgement is given. If you want to reproduce the whole article in a third-party publication (excluding your thesis/dissertation for which permission is not required) please go to the Copyright Clearance Center request page.

Read more about how to correctly acknowledge RSC content.

Social activity

Spotlight

Advertisements