Themed collection 2021 Inorganic Chemistry Frontiers HOT articles
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Blue-light-excited narrowing red photoluminescence in lead-free double perovskite Cs2−xKxAg0.6Na0.4In0.8Bi0.2Cl6−xBrx with cryogenic effects
The addition of KBr changed the original transition mode of the material and realized the blue-light excitation and narrow red emission of Cs2AgInCl6 at low temperatures.
Inorg. Chem. Front., 2022,9, 1879-1889
https://doi.org/10.1039/D1QI00928A
Two molybdenyl carbonates with different dimensional structures exhibiting huge differences in band gaps
Two molybdenyl carbonates with different dimensional structures exhibit huge differences in band gaps, 0D Cs3MoO4(HCO3) exhibiting a much larger band gap than 1D Cs2MoO3(CO3).
Inorg. Chem. Front., 2022,9, 440-447
https://doi.org/10.1039/D1QI01366A
Highly selective ethenolysis with acyclic-aminooxycarbene ruthenium catalysts
Acyclic carbene–ruthenium catalysts were developed for the ethenolysis. Remarkable catalytic efficiency (turnover numbers of 100 000) and excellent α-olefin selectivity (up to 98%) were exhibited.
Inorg. Chem. Front., 2022,9, 323-331
https://doi.org/10.1039/D1QI01132D
Distinct nonlinear optical responses in three pairs of 2D homochiral Ag(I) enantiomers modulated by dicarboxylic acid ligands
Based on three pairs of 2D homochiral Ag(I) enantiomers, we demonstrate that both the symmetry and degree of π-conjugation of the ligands have a significant effect on the type and intensity of their NLO responses.
Inorg. Chem. Front., 2022,9, 284-293
https://doi.org/10.1039/D1QI01321A
Synthesis of NaBH4 as a hydrogen carrier from hydrated borax using a Mg–Al alloy
We report a highly efficient synthesis of NaBH4 by optimizing the uses of a hydrogen source and low-cost Mg–Al alloy.
Inorg. Chem. Front., 2022,9, 370-378
https://doi.org/10.1039/D1QI01247A
Controlling the band structure and photocatalytic performance of single atom Ag/C3N4 catalysts by variation of silver concentration
We have investigated the effect of the concentration of single Ag atoms on the electronic structure of C3N4, and the relationship between the energy band structure and photocatalytic performance has been analysed in depth as well.
Inorg. Chem. Front., 2022,9, 302-309
https://doi.org/10.1039/D1QI01138C
The modification effect of Fe2O3 nanoparticles on ZnO nanorods improves the adsorption and detection capabilities of TEA
The depletion layer and more active sites are the key factors for improving the gas sensitivity of an Fe2O3/ZnO sensor.
Inorg. Chem. Front., 2022,9, 259-266
https://doi.org/10.1039/D1QI01339D
Self-reconstruction of cationic activated Ni-MOFs enhanced the intrinsic activity of electrocatalytic water oxidation
Here, the cation modified Ni-MOFs catalysts was cleverly designed. And the multilayer FeNi-LDH with enrich active sites derived by in-situ self-reconstruction in alkali solution was considered to be the decisive factor driving the OER reaction.
Inorg. Chem. Front., 2022,9, 179-185
https://doi.org/10.1039/D1QI00857A
Phosphomolybdic acid encapsulated in ZIF-8-based porous ionic liquids for reactive extraction desulfurization of fuels
Phosphomolybdic acid was encapsulated within a ZIF-8-based porous ionic liquid (HPMo@ZIF-8-PIL) for ultradeep reactive extraction desulfurization.
Inorg. Chem. Front., 2022,9, 165-178
https://doi.org/10.1039/D1QI01255J
Construction of brown mesoporous carbon nitride with a wide spectral response for high performance photocatalytic H2 evolution
A novel brown mesoporous carbon nitride photocatalyst is synthesized by a doping strategy. The excellent visible light response and stable mesoporous structure lead to an efficient hydrogen evolution activity.
Inorg. Chem. Front., 2022,9, 103-110
https://doi.org/10.1039/D1QI01137E
Photoactive perylenediimide metal–organic framework for boosting iodoperfluoroalkylation of alkenes and oxidative coupling of amines
A novel photoactive MOF was prepared based on an electron-deficient perylenediimide derivative, which exhibits excellent photocatalytic activities towards the iodoperfluoroalkylation of alkenes and the oxidation of amines to imines.
Inorg. Chem. Front., 2022,9, 111-118
https://doi.org/10.1039/D1QI01206A
Intramolecular π-conjugated channel expansion achieved by doping cross-linked dopants into carbon nitride frameworks for propelling photocatalytic hydrogen evolution and mechanism insight
PYM as a cross-linked bridge in CN frameworks via a multi-bonding mode expedites the transfer and separation of intramolecular photoproduced electron–hole pairs by π-conjugated channel expansion to improve the PHE activity.
Inorg. Chem. Front., 2022,9, 60-69
https://doi.org/10.1039/D1QI01122G
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Gating the photoactivity of azobenzene-type ligands trapped within a dynamic system of an M4L6 tetrahedral cage, an M2L2 metallocycle and mononuclear MLn complexes
Complexation of metal ions by a ligand bearing a azobenzene linker yielded two types of complexes: an [M2L2]4+ metallocycle and an [M4L6]8+ tetrahedral cage, which can be further converted into libraries of mononuclear [M(L′/L′′)n]2+ species.
Inorg. Chem. Front., 2021,8, 5195-5200
https://doi.org/10.1039/D1QI01063H
Broadband near-infrared BaMSi3O9:Cr3+ (M = Zr, Sn, Hf) phosphors for light-emitting diode applications
Cr3+-Doped BaMSi3O9 (M = Zr, Sn, Hf) NIR-emitting phosphors have been developed, which exhibit a broad NIR emission band over 650–1200 nm with a tunable band maximum longer than 800 nm and a FWHM of more than 155 nm upon blue light excitation.
Inorg. Chem. Front., 2021,8, 5186-5194
https://doi.org/10.1039/D1QI01082D
Deeply reduced empty Keggin clusters [MoIVxMVI12−xO40−xpyx] (x = 3, 6; M = Mo, W; py = pyridine): synthesis, structures, and Lewis field catalysis
First MoIV3-Keggin anions [MoIVxMVI12−xO40−xpyx]8− (M = Mo, W; x = 3, 6) display unprecedented empty Keggin structure caused by the weak u3-O coordinating capability of the [MoIV3O4] triads and LCF-dependent hydrogen transfer catalysis.
Inorg. Chem. Front., 2021,8, 5178-5185
https://doi.org/10.1039/D1QI01080H
Construction of a superhydrophobic microenvironment via polystyrene coating: an unexpected way to stabilize CuI against oxidation
A superhydrophobic microenvironment in MIL-101(Cr) was constructed via coating polystyrene, resulting in improved CuI stability and adsorptive desulfurization performance.
Inorg. Chem. Front., 2021,8, 5169-5177
https://doi.org/10.1039/D1QI01050F
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Aufbau vs. non-Aufbau ground states in two-coordinate d7 single-molecule magnets
Magnetic anisotropy is generated in two related d7 single-molecule magnets; (1) via 3d-4s orbital mixing in FeI; and (2) a non-Aufbau ground state in CoII, demonstrating that the electronic configurations are large retained independent of geometry.
Inorg. Chem. Front., 2021,8, 5076-5085
https://doi.org/10.1039/D1QI00912E
A binary all-nanoporous composite membrane constructed via vapor phase transformation for high-permeance gas separation
A COF with a large pore size was incorporated into a MOF matrix to construct an all-nanoporous composite membrane for high-permeance gas separation.
Inorg. Chem. Front., 2021,8, 5016-5023
https://doi.org/10.1039/D1QI00847A
Unprecedented icosahedral clusters built of polyantimony: from single [Ni0.5@{Sb6Ni6(CO)8}]4− and [Ni@{Sb7Ni5(CO)6}]3− to the Sb84−-linked dimer [(Sb8){Sb7Ni5(CO)4}2]6−
First icosahedral clusters built of polyantimony were prepared from the reactions of K2ZnSb and Ni(CO)2(PPh3)2. Sb84−-linked dimer provides a new way of thinking for the synthesis of hybrid clusters datively coordinated by polydentate Zintl anions.
Inorg. Chem. Front., 2021,8, 5086-5092
https://doi.org/10.1039/D1QI00872B
Photoinduced versus spontaneous host–guest electron transfer within a MOF and chromic/luminescent response
The MOF shows charge-transfer sensitized Eu(III) emission and spontaneous/photoinduced guest-to-host electron transfer, which allow chromic and luminescent sensing of NH3 (luminescence turn-off) and O2 (luminescence turn-on).
Inorg. Chem. Front., 2021,8, 4828-4837
https://doi.org/10.1039/D1QI01079D
Probing the generality of spin crossover complex T½vs. ligand 15N NMR chemical shift correlations: towards predictable tuning
A study of 6 families (42 members) demonstrates that within a family the easily calculated 15N-NMR values of ligands enable predictable tuning of T1/2 in the corresponding complexes, except for 2 families with weakly influencing meta-substituents.
Inorg. Chem. Front., 2021,8, 4846-4857
https://doi.org/10.1039/D1QI00919B
Dielectric switching, SHG response and Pd(II) adsorption of a multifunctional phase-transition complex
One-dimensional coordination polymer [(C2H4OH)C4H9NS]CdCl3 has the performance of dielectric switching and SHG response. And the compound can adsorb precious Pd(II) and the adsorption could be monitored by dielectric anomaly and SHG signal.
Inorg. Chem. Front., 2021,8, 4858-4863
https://doi.org/10.1039/D1QI01017D
Ba2Ge2Te5: a ternary NLO-active telluride with unusual one-dimensional helical chains and giant second harmonic-generation tensors
The linear-optical and NLO properties of a ternary NLO-active telluride, Ba2Ge2Te5, were investigated systematically at the experimental and theoretical levels for the first time.
Inorg. Chem. Front., 2021,8, 4838-4845
https://doi.org/10.1039/D1QI01012C
Pressure-dependent modifications in the optical and electronic properties of Fe(IO3)3: the role of Fe 3d and I 5p lone–pair electrons
The electronic and transport properties of Fe(IO3)3 have been characterized under compression. A nice correlation of bandgaps of iodates to orbital configuration is proposed giving an explanation for the 2.1 eV bandgap of Fe(IO3)3.
Inorg. Chem. Front., 2021,8, 4780-4790
https://doi.org/10.1039/D1QI00870F
Heterogeneous interface design of bimetallic selenide nanoboxes enables stable sodium storage
The heterostructure SnSe2/CoSe2 core encapsulated in a carbon nanobox shell guarantees the structural stability and further ensures stable high performance for sodium ion batteries.
Inorg. Chem. Front., 2021,8, 4796-4805
https://doi.org/10.1039/D1QI00962A
Construction of a new Au27Cd1(SAdm)14(DPPF)Cl nanocluster by surface engineering and insight into its structure–property correlation
Surface engineering with a functional DPPF ligand and Cd atom is employed on a Au38 nanocluster to obtain a Au–Cd alloy nanocluster, that is, Au27Cd1. The difference in properties between Au38 and Au27Cd1 indicates the importance of the surface structure.
Inorg. Chem. Front., 2021,8, 4820-4827
https://doi.org/10.1039/D1QI01015H
Optimizing the relaxivity at high fields: systematic variation of the rotational dynamics in polynuclear Gd-complexes based on the AAZTA ligand
A homogeneous series of polynuclear Gd-complexes (n = 1–8) based on a stable and bis-hydrated [Gd(AAZTA)]− chelate shows high relaxivity values at high fields (1.5–7 T), per Gd, particularly pronounced for the more rigid and compact members.
Inorg. Chem. Front., 2021,8, 4806-4819
https://doi.org/10.1039/D1QI00904D
Two deep-ultraviolet nonlinear optical monolayers obtained by a template-optimized design strategy
We obtained two two-dimentional deep-ultraviolet nonlinear optical layers with a large band gap and proper second harmonic generation by a template-optimized design strategy.
Inorg. Chem. Front., 2021,8, 4791-4795
https://doi.org/10.1039/D1QI00945A
A photoactivated Ir(III) complex targets cancer stem cells and induces secretion of damage-associated molecular patterns in melanoma cells characteristic of immunogenic cell death
The new iridium complex selectively targets cancer stem cells and has potential to induce immunogenic cell death in cancer cells.
Inorg. Chem. Front., 2021,8, 4696-4711
https://doi.org/10.1039/D1QI00856K
A biodegradable bismuth–gadolinium-based nano contrast agent for accurate identification and imaging of renal insufficiency in vivo
A biodegradable gadolinium-doped mesoporous bismuth-based nanomaterial is used to diagnose kidneys with dysfunction accurately via magnetic resonance imaging in vivo.
Inorg. Chem. Front., 2021,8, 4720-4729
https://doi.org/10.1039/D1QI00878A
A data-driven approach to predicting band gap, excitation, and emission energies for Eu2+-activated phosphors
An integrated ML model platform is developed to predict the peak emission wavelength (PEW), excitation band edge wavelength (EBEW), and band gap (Eg) from structural, elemental, chemical, and physical descriptors of Eu2+-activated phosphors.
Inorg. Chem. Front., 2021,8, 4610-4624
https://doi.org/10.1039/D1QI00766A
Anderson-type polyoxometalate-based complexes constructed from a new ‘V’-like bis-pyridine–bis-amide ligand for selective adsorption of organic dyes and detection of Cr(VI) and Fe(III) ions
Four isostructural complexes constructed from Anderson-type POM and new ‘V’-like ligands exhibited outstanding selective adsorption capacities for organic dyes, and electrochemical sensing behaviors toward Cr(VI) and Fe(III) ions.
Inorg. Chem. Front., 2021,8, 4458-4466
https://doi.org/10.1039/D1QI00785H
Novel noncentrosymmetric polar coordination compounds derived from chiral histidine ligands
Noncentrosymmetric chiral Zn- and Cd-coordination compounds have been synthesized by a slow evaporation method using histidine under acidic conditions.
Inorg. Chem. Front., 2021,8, 4536-4543
https://doi.org/10.1039/D1QI00869B
Na1.5Rb0.5PO3F·H2O: synthesis, properties, and stepwise reconstruction of the hydrogen bond network
The precise substitution of NH4+ with Na+/Rb+ cations in NPF·H2O leads to a stepwise reconstruction of the hydrogen bond networks from NPF·H2O, NNPF·H2O to NRPF·H2O, giving rise to the symmetry and optical property tunings.
Inorg. Chem. Front., 2021,8, 4544-4552
https://doi.org/10.1039/D1QI00895A
A new tunnel-type V4O9 cathode for high power density aqueous zinc ion batteries
A mixed-valence vanadium oxide V4O9 with a tunnel structure was synthesized as a cathode material for aqueous zinc ion batteries. A Zn//V4O9 battery displays high specific capacity and excellent rate performance.
Inorg. Chem. Front., 2021,8, 4497-4506
https://doi.org/10.1039/D1QI00747E
Olivine-type cadmium germanate: a new sensing semiconductor for the detection of formaldehyde at the ppb level
In this study, for the first time, olivine-structured Cd2GeO4 was identified as an excellent formaldehyde sensing material, with a low detection limit of 60 ppb.
Inorg. Chem. Front., 2021,8, 4467-4473
https://doi.org/10.1039/D1QI00772F
Ultrasonic assisted exfoliation for efficient production of RuO2 monolayer nanosheets
RuO2 monolayer nanosheets can be easily synthesized by an ultrasonic assisted exfoliation process.
Inorg. Chem. Front., 2021,8, 4482-4487
https://doi.org/10.1039/D1QI00652E
Tandem-like vanadium cluster chains in a polyoxovanadate-based metal–organic framework for efficient catalytic oxidation of sulfides
The vanadium cluster chain in V-Ni-MOF can efficiently catalyze the oxidation of sulfides with hydrogen peroxide as the oxidant, achieving the complete conversion from sulfides to sulfones within 1 hour at 40 °C.
Inorg. Chem. Front., 2021,8, 4367-4375
https://doi.org/10.1039/D1QI00799H
Structural determination of a metastable Ag27 nanocluster and its transformations into Ag8 and Ag29 nanoclusters
The atomically precise structure of a metastable nanocluster, Ag27H11(SPhMe2)12(DPPM)6, was determined, and its transformations into size-reduction Ag8 and size-growth Ag29 nanoclusters have been mapped out.
Inorg. Chem. Front., 2021,8, 4407-4414
https://doi.org/10.1039/D1QI00684C
Synthesis of 3D flower-like hierarchical NiCo-LDH microspheres with boosted electrochemical performance for hybrid supercapacitors
3D flower-like NiCo-LDH microspheres synthesized via conformal alkaline hydrolysis strategy possess superior specific capacitance and stability, and the assembled HSC exhibits prominent power/energy density and durability.
Inorg. Chem. Front., 2021,8, 4324-4333
https://doi.org/10.1039/D1QI00613D
Carbon coated SiO nanoparticles embedded in hierarchical porous N-doped carbon nanosheets for enhanced lithium storage
Carbon coated SiO nanoparticles embedded in N-doped carbon nanosheets were synthesized via a scalable and cost-effective route, and exhibited enhanced cyclability and rate capability as an anode for lithium-ion batteries.
Inorg. Chem. Front., 2021,8, 4282-4290
https://doi.org/10.1039/D1QI00778E
Alkali-regulated Fe6 and Fe18 molecular clusters and their structural transformation
A cyclic Fe6 like a “six-vane windmill” and a bricky Fe18 clusters as a “Chinese knot” were obtained. Moreover, the alkali-induced conversion from Fe6 to Fe18 has been achieved, realizing the nuclearity enlargement and structural regulation.
Inorg. Chem. Front., 2021,8, 4186-4191
https://doi.org/10.1039/D1QI00750E
Extraction of the trivalent transplutonium actinides americium through einsteinium by the sulfur donor Cyanex 301
When extracting metals with the sulfur donor ligand, Cyanex 301 (bis(2,4,4-trimethylpentyl)dithiophosphinic acid), a transition in the coordination mode of extracted complexes has been observed between Eu and Gd, but not within the actinide series.
Inorg. Chem. Front., 2021,8, 4177-4185
https://doi.org/10.1039/D1QI00076D
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A bifunctional robust metal sulfide with highly selective capture of Pb2+ ions and luminescence sensing ability for heavy metals in aqueous media
A 3-D metal sulfide ion exchanger (MSIE) with extra-framework H+ ions showed a remarkable capability for sorption of Pb2+ ions and highly efficient luminescence sensing properties towards various heavy metal ions.
Inorg. Chem. Front., 2021,8, 4052-4061
https://doi.org/10.1039/D1QI00666E
Rational assembly of metal-oxo clusters into molecular materials via a “wheel mounting” mode
Presented here is the self-assembly of metal-oxo clusters into molecular materials of different shapes and sizes via a “wheel mounting” mode, and molecular transformation was optical-driven.
Inorg. Chem. Front., 2021,8, 4102-4106
https://doi.org/10.1039/D1QI00779C
Pb2.28Ba1.72B10O19 featuring a three-dimensional B–O anionic network with edge-sharing [BO4] obtained under ambient pressure
The unique borate Pb2.28Ba1.72B10O19 containing a three-dimensional B–O anionic network with edge-sharing [BO4] was obtained under ambient pressure, featuring an extremely large B–B interatomic distance (dB–B) and small internal O–B–O angles (∠in(O–B–O)).
Inorg. Chem. Front., 2021,8, 3716-3722
https://doi.org/10.1039/D1QI00653C
K2Pb(H2C3N3O3)4(H2O)4: a potential UV nonlinear optical material with large birefringence
K2Pb(H2C3N3O3)4(H2O)4 (I) features a 2D [K2PbO8(H2O)4]12- anionic layer and reveals a moderate SHG signal of approximately 2.6 × KDP.
Inorg. Chem. Front., 2021,8, 3547-3555
https://doi.org/10.1039/D1QI00595B
A stable mixed-valent uranium(V,VI) organic framework as a fluorescence thermometer
A stable mixed-valent uranium(V/VI) organic framework with a 3D interpenetrating structure was synthesized, which can be used as a dual-responsive fluorescence temperature sensor based on the fluorescence intensity and fluorescence lifetime.
Inorg. Chem. Front., 2021,8, 3514-3521
https://doi.org/10.1039/D1QI00580D
Defect-boosted molybdenite-based co-catalytic Fenton reaction
High-defect molybdenite acts an efficient co-catalyst to substantially enhance the Fenton reaction.
Inorg. Chem. Front., 2021,8, 3440-3449
https://doi.org/10.1039/D1QI00344E
An Al–Li alloy/water system for superior and low-temperature hydrogen production
A superior and low-temperature hydrogen supply technology based on the hydrolysis of an Al–Li alloy was developed.
Inorg. Chem. Front., 2021,8, 3473-3481
https://doi.org/10.1039/D1QI00487E
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M/TiO2 (M = Fe, Co, Ni, Cu, Zn) catalysts for photocatalytic hydrogen production under UV and visible light irradiation
Cu/TiO2 photocatalysts can be considered a promising low-cost alternative to the well-known Pt/TiO2 system for hydrogen production under UV-Vis irradiation.
Inorg. Chem. Front., 2021,8, 3491-3500
https://doi.org/10.1039/D0QI01311K
Designing lanthanide coordination nanoframeworks as X-ray responsive radiosensitizers for efficient cancer therapy
A series of three-dimensional Ln-based coordination nanoframeworks were designed and shown potential as efficient and low toxic X-ray responsive radiosensitizers for the treatment of cervical cancer.
Inorg. Chem. Front., 2021,8, 3433-3439
https://doi.org/10.1039/D1QI00442E
Polyoxometalate modified transparent metal selenide counter electrodes for high-efficiency bifacial dye-sensitized solar cells
We present a facile one-step hydrothermal approach for the growth of PW11Co/Co0.85Se on a conductive glass substrate, which could be used as transparent CE in bifacial DSSCs with enhanced front and back efficiencies of 7.56% and 5.82%, respectively.
Inorg. Chem. Front., 2021,8, 3230-3237
https://doi.org/10.1039/D1QI00447F
Stepwise coordination isomerism of 2D networks: adsorption of diiodomethane into crystals and recognition in SCSC mode
3CH2Cl2·2C2H5OH@[CdI2L] with a new 2D topology of {43·62·8} are isomerized into new single crystals of 4C4H8O@[CdI2L]. Interestingly, both crystals are integral to an efficient and tolerant matrix for recognition of diiodomethane in the SCSC mode.
Inorg. Chem. Front., 2021,8, 3292-3300
https://doi.org/10.1039/D1QI00540E
A hydrogen evolution catalyst lowering energy consumption in aluminum anodization
Aluminum anodization process requires a lot of electrical energy for the migration of ions in a barrier-type oxide film, in which electrode polarization leads to massive energy consumption.
Inorg. Chem. Front., 2021,8, 3284-3291
https://doi.org/10.1039/D1QI00377A
Low-cost and multi-level structured NiFeMn alloy@NiFeMn oxyhydroxide electrocatalysts for highly efficient overall water splitting
NiFeMn alloy@NiFeMn oxyhydroxide was fabricated by electrodeposition, which reveals exceptional electrocatalytic property toward overall water splitting owing to the extraordinary multi-level structure.
Inorg. Chem. Front., 2021,8, 2713-2724
https://doi.org/10.1039/D1QI00215E
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Unprecedented collateral sensitivity for cisplatin-resistant lung cancer cells presented by new ruthenium organometallic compounds
Ru compounds exhibit collateral sensitivity in cisplatin-resistant NSCLC and increase cisplatin activity by inhibiting efflux pumps.
Inorg. Chem. Front., 2021,8, 1983-1996
https://doi.org/10.1039/D0QI01344G
Fabrication of 2D/2D COF/SnNb2O6 nanosheets and their enhanced solar hydrogen production
2D TpPa-2-COF tightly decorated on the surface of SnNb2O6 nanosheets effectively increases the interface region, promotes separation of carriers and heightens charge utilization rate, thus achieving better solar H2-production activity than bare SnNb2O6 and TpPa-2-COF.
Inorg. Chem. Front., 2021,8, 1686-1694
https://doi.org/10.1039/D0QI01443E
Hierarchical interlayer-expanded MoSe2/N–C nanorods for high-rate and long-life sodium and potassium-ion batteries
The hierarchical structure and N-doped carbon coating buffer the volume expansion and maintain the structure integrity of MoSe2, which enables the long cycle performance and high rate capability for both sodium and potassium storage.
Inorg. Chem. Front., 2021,8, 1271-1278
https://doi.org/10.1039/D0QI01340D
About this collection
Read our on-going collection of the hottest research published as advanced article from Inorganic Chemistry Frontiers in 2021. These articles are recommended by reviewers as being of significant novelty and interest. Congratulations to all the authors whose articles are featured!