Issue 7, 2023

Synchrotron radiation based operando characterization of battery materials

Abstract

Synchrotron radiation based techniques are powerful tools for battery research and allow probing a wide range of length scales, with different depth sensitivities and spatial/temporal resolutions. Operando experiments enable characterization during functioning of the cell and are thus a precious tool to elucidate the reaction mechanisms taking place. In this perspective, the current state of the art for the most relevant techniques (scattering, spectroscopy, and imaging) is discussed together with the bottlenecks to address, either specific for application in the battery field or more generic. The former includes the improvement of cell designs, multi-modal characterization and development of protocols for automated or at least semi-automated data analysis to quickly process the huge amount of data resulting from operando experiments. Given the recent evolution in these areas, accelerated progress is expected in the years to come, which should in turn foster battery performance improvements.

Graphical abstract: Synchrotron radiation based operando characterization of battery materials

Article information

Article type
Perspective
Submitted
07 Aug. 2022
Accepted
11 Dec. 2022
First published
12 Dec. 2022
This article is Open Access

All publication charges for this article have been paid for by the Royal Society of Chemistry
Creative Commons BY-NC license

Chem. Sci., 2023,14, 1641-1665

Synchrotron radiation based operando characterization of battery materials

A. P. Black, A. Sorrentino, F. Fauth, I. Yousef, L. Simonelli, C. Frontera, A. Ponrouch, D. Tonti and M. R. Palacín, Chem. Sci., 2023, 14, 1641 DOI: 10.1039/D2SC04397A

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