Issue 25, 2015
From the journal:

Chemical Communications

Assessing dimerisation degree and cooperativity in a biomimetic small-molecule model by pulsed EPR†

K. Ackermann,a   A. Giannoulis,a   D. B. Cordes,a   A. M. Z. Slawina  and  B. E. Bode*a  

* Corresponding authors

a EaStCHEM School of Chemistry, Biomedical Sciences Research Complex and Centre of Magnetic Resonance, University of St Andrews, North Haugh, St Andrews KY16 9ST, UK
E-mail: beb2@st-andrews.ac.uk

Abstract

Pulsed electron paramagnetic resonance (EPR) spectroscopy is gaining increasing importance as a complementary biophysical technique in structural biology. Here, we describe the synthesis, optimisation, and EPR titration studies of a spin-labelled terpyridine Zn(II) complex serving as a small-molecule model system for tuneable dimerisation.

Graphical abstract: Assessing dimerisation degree and cooperativity in a biomimetic small-molecule model by pulsed EPR

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DOI
https://doi.org/10.1039/C4CC08656B
Article type
Communication
Submitted
31 10 2014
Accepted
08 1 2015
First published
08 1 2015
This article is Open Access
Creative Commons BY license

Chem. Commun., 2015,51, 5257-5260

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Assessing dimerisation degree and cooperativity in a biomimetic small-molecule model by pulsed EPR

K. Ackermann, A. Giannoulis, D. B. Cordes, A. M. Z. Slawin and B. E. Bode, Chem. Commun., 2015, 51, 5257 DOI: 10.1039/C4CC08656B

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