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We report an alternating-reduction approach by galvanic replacement and co-reduction to enable incorporation of Pd into Pt shell, and the obtained PtPd hollow nanocubes with an enhanced alloy effect and highly active {100} facets show high catalytic activity and superior durability in the methanol oxidation reaction.

Graphical abstract: PtPd hollow nanocubes with enhanced alloy effect and active facets for efficient methanol oxidation reaction

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